Supporting data for "Synthesis of Singly Threaded High-order Rotaxanes and Investigation on Their Potential in Radial High-order Catenane Assembly"

The project focuses on the synthesis of high-order rotaxane and its potential as a precursor for high-order catenane assembly. This dataset includes the ¹H NMR, ¹³C{¹H} NMR, ¹H-¹H COSY and 2D NOESY spectra, and HR-ESI-MS spectra for hetero[3]-, [4]-, [5]- and [6]rotaxanes synthesized. The ¹H NMR spectra of the preliminary study on the catenane assembly are included in the dataset as well.